Experimental Details: In duplicate in a 4-ml vial equipped with a teflon septa and 2x7 mm stir bar, were weighed 4-bromoacetophenone (4.95 mg, 25 μmol) and potassium benzyltrifluoroborate (4.50 mg, 25 μmol, 1 equiv.). To this vial was added a 1.0 ml solution in DMA containing NiCl2-dme (1.1…

The EvoluChem™ PhotoRedOx Box device is designed to facilitate photochemical experiment. This device is compatible with most vial formats (0.3 ml, 2 ml, 4 ml and 20 ml vials). Its compact design allows for use with any stirring plate. A built-in fan keeps the reaction conditions at room…