The EvoluChem™ PhotoRedOx Box device is designed to facilitate photochemical experiment. This device is compatible with most vial formats (0.3 ml, 2 ml, 4 ml and 20 ml vials). Its compact design allows for use with any stirring plate. A built-in fan keeps the reaction conditions at room temperature. (Patent Pending)
Features:
- Light source (kessil blue 34W), other sources can be adapted
- Photochemistry chamber to evenly distribute light
- Flexible format vials
- Magnetic stirring on standard heat/stirring plate
- Cooling by fan to maintain experiment at room temperature
- Pre-designed array of catalysts and reagents available
Benefits:
- Easy setup on a standard stirring plate
- Perform up to 32 reaction conditions simultaneously
- Individually sealed vials enable flexible study design
- Save your substrate using low scale reaction conditions
- Save time on optimization
PhotoRedOx Flow Reactor
The common limitation to scaling up photoredox chemistry is due to the low penetration of the light in to the reaction mixture (few mm) which prohibits the use of large reaction vessels. Surface area is key to shorten reaction time. It is possible to significantly increase the surface area by running the reaction in flow. This will decreases the reaction time and allows to be run in continuous mode for scale-up. To solve this challenge, we designed a flow reactor that can be used in the PhotoRedOx Box.
This flow reactor is using PFA tubing and has volume of 2mL. Comparing reactions in flow and in batch we observed significant decrease in reaction time.
PhotoRedOx Duo
The EvoluChem™ PhotoRedOx Duo is using the same unique design as the PhotoRedOx Box. PhotoRedOx Duo increases the reaction vials capacity to 16 vials (2, 4 or 8 ml) using 2 of the same vial holders as the PhotoRedOx box. Using the 2 blue LED setup allows to increase reaction rate of difficult reaction conditions.